(E)-1-[1-(4-Chlorophenyl)ethylidene]thiosemicarbazide
نویسندگان
چکیده
In the crystal structure of the title compound, C(9)H(10)ClN(3)S, the mol-ecules form chains parallel to [001] through N-H⋯S hydrogen bonds. In addition, weak inter-molecular N-H⋯Cl hydrogen bonds connect the chains, forming a two-dimensional network parallel to (001).
منابع مشابه
1-[1-(4-Nitrophenyl)ethylidene]thiosemicarbazide
The title compound, C(9)H(10)N(4)O(2)S, was prepared by the reaction of 1-(4-nitro-phen-yl)ethanone and thio-semicarbazide in ethanol at 367 K. There are weak inter-molecular N-H⋯S and N-H⋯O hydrogen-bonding inter-actions in the crystal structure involving the amine and nitrile groups, respectively, as donors.
متن کاملN′-[1-(4-Chlorophenyl)ethylidene]acetohydrazide
In the title compound, C(10)H(11)ClN(2)O, the dihedral angle between the acetohydrazide group and the aromatic ring is 33.76 (9)°. In the crystal, inversion dimers linked by pairs of N-H⋯O hydrogen bonds generate R(2) (2)(8) loops.
متن کاملIodido{4-phenyl-1-[1-(1,3-thiazol-2-yl-κN)ethylidene]thiosemicarbazidato-κ2 N′,S}{4-phenyl-1-[1-(1,3-thiazol-2-yl)ethylidene]thiosemicarbazide-κS}mercury(II)
In the title compound, [Hg(C(12)H(11)N(4)S(2))I(C(12)H(12)N(4)S(2))], the Hg atom is in a distorted square-pyramidal coordination, defined by the iodide ligand, by the S atom of the neutral ligand in the apical position, and by the N atom of the thia-zole ring, the thio-ureido N and the S atom of the deprotonated ligand. The deprotonated ligand intra-molecularly hydrogen bonds to the thia-zole ...
متن کامل1-[1-(4-Bromophenyl)ethylidene]-4-(2,4-dimethoxyphenyl)thiosemicarbazide
In the title compound, C(17)H(18)BrN(3)O(2)S, the dihedral angle between the aromatic rings is 9.15 (17)°. A bifurcated intra-molecular N-H⋯(N,O) hydrogen bond generates two S(5) rings and a weak intra-molecular C-H⋯S inter-action completes an S(6) ring motif. In the crystal, inversion dimers linked by pairs of N-H⋯S hydrogen bonds generate R(2) (2)(8) loops and weak C-H⋯S and C-H⋯π inter-actio...
متن کامل1-[1-(4-Chlorophenyl)ethylidene]carbonohydrazide
The mol-ecular skeleton of the title mol-ecule, C(9)H(11)ClN(4)O, is essentially planar, the dihedral angle between the ring and the and N/N/C plane being 6.7 (3)°. In the crystal, inter-molecular N-H⋯O and N-H⋯N hydrogen bonds link the mol-ecules into ribbons propagated along [010].
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عنوان ژورنال:
دوره 68 شماره
صفحات -
تاریخ انتشار 2012